Shaw, Kailash Kumar and G, Satyanarayana
(2015)
Domino Jeffery Heck Reaction Followed by Aldol Condensation: An Efficient Strategy for the Synthesis of Functionalized A croleins.
Masters thesis, Indian Institute of Technology Hyderabad.
Abstract
Synthetic protocols like domino or sequential one-pot are considered to be valuable techniques in organic synthesis as they are devoid of intermediate isolation.1 These one-pot processes involve multiple steps to be catalysed sequentially by a metal complex or sequential addition of reagents to drive a set of reactions. In recent years the transition metal catalysis mainly that of palladium and copper are found to be the most powerful platform in order to perform such kind of transformations. Taking this advantage of transition metals, in the present context we have described a few efficient strategies for the synthesis of substituted acroleins from the simple and readily accessible iodoarenes and allylic alcohols by using palladium acetate and triethylamine as catalyst and base respectively.
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