Single‐Column‐Based Heck Coupling, Condensation and Alkylation Strategy: Synthesis of 2‐Benzoyl‐2‐alkyl‐2,3‐dihydro‐1 H ‐inden‐1‐ones

Dorjay Lama, Penang and Bhaskara Rao, Latchipatula and Sreenivasulu, Chinnabattigalla and Ravi Kishore, Dakoju and Satyanarayana, G. (2021) Single‐Column‐Based Heck Coupling, Condensation and Alkylation Strategy: Synthesis of 2‐Benzoyl‐2‐alkyl‐2,3‐dihydro‐1 H ‐inden‐1‐ones. ChemistrySelect, 6 (46). pp. 13041-13045. ISSN 2365-6549

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Abstract

An efficient method for the synthesis of alkyl benzoyl indanones via a simple intermolecular Heck coupling followed by intramolecular condensation, and alkylation is presented. Notably, the strategy exhibited good substrate scope and enabled the synthesis of diverse alkyl substituted 1,3-dicarbonyl products. Significantly, this protocol was successful using a single-column purification technique. © 2021 Wiley-VCH GmbH

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IITH Creators:

IITH Creators	ORCiD
Satyanarayana, G.	UNSPECIFIED

Item Type:

Article

Additional Information:

. We are grateful to the Department of Science and Technology Science and Engineering Research Board (DST‐SERB) [No. EMR/2017/005312], New Delhi, for financial support. C. B. S & D. R thanks UGC for the award of the research fellowship

Uncontrolled Keywords:

1,3 Di-ketone; Alkyl benzoyl indanones; Heck Coupling; Intramolecular Condensation; Single-column

Subjects:

Chemistry

Divisions:

Department of Chemistry

Depositing User:

. LibTrainee 2021

Date Deposited:

26 Sep 2022 09:12

Last Modified:

26 Sep 2022 09:12